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JSSS | Articles | Volume 7, issue 2
J. Sens. Sens. Syst., 7, 621-625, 2018
https://doi.org/10.5194/jsss-7-621-2018
© Author(s) 2018. This work is distributed under
the Creative Commons Attribution 4.0 License.

Special issue: Sensors and Measurement Systems 2018

J. Sens. Sens. Syst., 7, 621-625, 2018
https://doi.org/10.5194/jsss-7-621-2018
© Author(s) 2018. This work is distributed under
the Creative Commons Attribution 4.0 License.

Regular research article 06 Dec 2018

Regular research article | 06 Dec 2018

Highly sensitive coulometric titration of oxygen for the characterization of solid materials at elevated temperatures

Alexander Herms et al.
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Cited articles  
Fouletier, J., Vitter, G., and Kleitz, M.: Measurement and regulation of oxygen content in gases using solid electrolyte cells, III, Oxygen pump-gauge, J. Appl. Electrochem., 5, 111–120, https://doi.org/10.1007/BF00613213, 1975. 
Sahibzada, M., Mantzavinos, D., Hartley, A., Morton, W., and Metcalfe, I. S.: Solid Electrolyte Coulometric Studies of Oxide State and Kinetics, Chem. Eng. Res. Des., 78, 965–970, https://doi.org/10.1205/026387600528229, 2000. 
Schelter, M., Zosel, J., Oelßner, W., Guth, U., and Mertig, M.: A solid electrolyte sensor for trace gas analysis, Sensor Actuat. B-Chem., 187, 209–214, https://doi.org/10.1016/j.snb.2012.10.111, 2013. 
Schelter, M., Zosel, J., Oelßner, W., and Mertig, M.: A novel method for measuring dissolved gases in liquids, Sensor Actuat. B-Chem., 193, 113–120, https://doi.org/10.1016/j.snb.2013.11.070, 2014. 
Schelter, M., Zosel, J., Vashook, V., Guth, U., Oelßner, W., and Mertig, M.: Trace gas measurements with zirconia sensors: An overview, in: Sensors and Electronic Instrumentation Advances: Proceedings of the 2nd International Conference on Sensors Engineering and Electronics Instrumental Advances (SEIA' 2016), 22–23 September, Barcelona, Spain, 2016. 

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For the understanding of new materials, especially oxides, oxygen exchange of such materials and its consequences for their properties are of high interest. For this purpose a new setup for oxygen solid electrolyte coulometry with electrochemical cells made of yttria-stabilized zirconia (YSZ) is presented. It could be shown that this setup enables the measurement of exchanged oxygen from the picomol up to the higher nanomol range with a precision which was not achieved so far.
For the understanding of new materials, especially oxides, oxygen exchange of such materials and...
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